2-(2-甲基苯基)苯乙酮合成路线 （共 22 条）
反应条件
potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
0.75 h; Heating;
参考文献
Hamann, Blake C.; Hartwjg, John F.
Journal of the American Chemical Society, 1997 , vol. 119, # 50 p. 12382 - 12383
反应条件
(C5H5)Fe(C5H3C(CH3)NC6H4CH3)PdCl(CN2(C6H3(CH(CH3)2)2)2C2H2); potassium tert-butylate in toluene
2 h; Inert atmosphereReflux;
参考文献
Zhang, Jinli; Yang, Xueqian; Cui, Xiuling; Wu, Yangjie
Tetrahedron, 2011 , vol. 67, # 45 p. 8800 - 8807
反应条件
water; PtCl4-CO in tetrahydrofuran
T=80°C; P=1034.3 Torr; 3 h;
参考文献
Baidossi, Wael; Lahav, Michal; Blum, Jochanan
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 669 - 672
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=130°C; Heck reaction; 20 h;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran
T=80°C; 3 h; Schlenk tubeInert atmosphere;
参考文献
Rao, Maddali L.N.; Giri, Somnath; Jadhav, Deepak N.
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6133 - 6138
反应条件
1: sec-phenethyl alcohol With [Pd(η3-allyl)(Cl)((N,N′-bis-(2,6-diisopropylphenyl)imidazol-2-ylidene))]; 4-methyl-chlorobenzene; potassium tert-butylate in toluene
T=40°C; 3 h; Inert atmosphere;
2: ortho-chlorotoluene in toluene
T=80°C; 6 h; Inert atmosphere;
参考文献
Landers, Brant; Berini, Christophe; Wang, Chao; Navarro, Oscar
Journal of Organic Chemistry, 2011 , vol. 76, # 5 p. 1390 - 1397
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=80°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
反应条件
Ni(PCy3)2Cl2; sodium t-butanolate in N,N-dimethyl-formamide; toluene
T=100°C; Suzuki-Miyaura coupling; 1 h; Inert atmosphere;
参考文献
Huang, Kun; Li, Gang; Huang, Wei-Ping; Yu, Da-Gang; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 25 p. 7224 - 7226
反应条件
in diethyl ether
4 h; Heating;
参考文献
Wagner, Peter J.; Meador, Michael A.; Zhou, Boli; Park, Bong-Ser
Journal of the American Chemical Society, 1991 , vol. 113, # 25 p. 9630 - 9639
反应条件
aluminium trichloride
参考文献
Newman; Gaertner
Journal of the American Chemical Society, 1950 , vol. 72, p. 264,271
