4’-溴-2’-羟基-5’-甲基苯乙酮合成路线 （共 6 条）
反应条件
bromine in chloroform T=-12 - -10°C; 0.5 h;
参考文献
Gabriel, Gabriel; Pickles, Robert; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1989 , # 11 p. 2713 - 2739
反应条件
aluminium trichloride T=100 - 180°C; 0.166667 h;
参考文献
Gabriel, Gabriel; Pickles, Robert; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1989 , # 11 p. 2713 - 2739
反应条件
1: 50 percent / AlCl3 / temperature up to 150 deg C 2: 74.5 percent / Br2 / CHCl3 / 0.5 h / -12 - -10 °C View Scheme
参考文献
Gabriel, Gabriel; Pickles, Robert; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1989 , # 11 p. 2713 - 2739
反应条件
1: 26.9 percent / Br2 / CHCl3 / 0 - 5 °C 2: 2.56 g / conc. H2SO4 / 0.25 h 3: 80 percent / AlCl3 / 0.17 h / 100 - 180 °C View Scheme
参考文献
Gabriel, Gabriel; Pickles, Robert; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1989 , # 11 p. 2713 - 2739
反应条件
1: 2.56 g / conc. H2SO4 / 0.25 h 2: 80 percent / AlCl3 / 0.17 h / 100 - 180 °C View Scheme
参考文献
Gabriel, Gabriel; Pickles, Robert; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1989 , # 11 p. 2713 - 2739
反应条件
1: K2CO3 / acetone / 24 h / Heating 2: 56 percent / NaOEt / ethanol / 3 h / Ambient temperature 3: Cu powder / quinoline / 1 h / Heating View Scheme
参考文献
Gabriel, Gabriel; Pickles, Robert; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1989 , # 11 p. 2713 - 2739
