反应条件
n-butyl lithium in diethyl ether; hexane under Ar, addn. of n-butyl lithium (hexane) to the diene (ether) (-78°C, stirring, 2 h ), warming to room temp., recooling to -78°C, addn. to stilbine, stirring (20 min), warming to room temp.; solv. removed, extraction (pentane), recrystn. (pentane), elem. anal.;
参考文献
Ashe, Arthur J.; Kampf, Jeff W.; Al-Taweel, Samir M.
Organometallics, 1992 , vol. 11, p. 1491 - 1496
