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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
50361-53-0
合成路线
（共 25 条）
50361-53-0
→
反应条件
1335545-22-6
+
1335545-31-7
反应条件
1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 3: immobilized Pseudomonas cepacia lipase; water / diethyl ether / 16 h / 30 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1335545-23-7
+
529-34-0
1-四氢萘酮
反应条件
1.1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2.1: 4-(N,N-dimethlyamino)pyridine / ethyl acetate / 2 h / 20 °C / Inert atmosphere 3.1: immobilized Candida antarctica lipase A; water / 2-ethoxy-2-methylpropane / 168 h / Enzymatic reaction 3.2: 6 h / 20 °C View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1335545-31-7
+
529-34-0
1-四氢萘酮
反应条件
1.1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2.1: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 3.1: immobilized Candida antarctica lipase A; water / diethyl ether / 2 h / 30 °C / Enzymatic reaction 3.2: 6 h / 20 °C View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1092080-61-9
+
1335545-22-6
+
1335545-25-9
反应条件
1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 3: immobilized Candida antarctica lipase A; water / 1,4-dioxane / 144 h / 40 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1092080-61-9
+
1335545-22-6
+
1335545-26-0
+
1335545-25-9
+
529-34-0
1-四氢萘酮
反应条件
1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 3: immobilized Candida antarctica lipase A; water / tert-butyl methyl ether / 48 h / 40 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1092080-61-9
+
1335545-22-6
+
1335545-23-7
+
1335545-21-5
+
529-34-0
1-四氢萘酮
反应条件
1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2: 4-(N,N-dimethlyamino)pyridine / ethyl acetate / 2 h / 20 °C / Inert atmosphere 3: immobilized Candida antarctica lipase A; water / 2-ethoxy-2-methylpropane / 168 h / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1335545-25-9
反应条件
1.1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2.1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 3.1: immobilized Candida antarctica lipase A; water / 1,4-dioxane / 144 h / 40 °C / Enzymatic reaction 3.2: 6 h / 20 °C View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1092080-61-9
+
1335545-22-6
+
1335545-26-0
+
1335545-25-9
反应条件
1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 3: immobilized Candida antarctica lipase A; water / tetrahydrofuran / 168 h / 40 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1335545-25-9
反应条件
1.1: hydrogenchloride / dichloromethane; water; acetonitrile / 1 h / 20 °C 2.1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 3.1: immobilized Candida antarctica lipase A; water / tetrahydrofuran / 168 h / 40 °C / Enzymatic reaction 3.2: 6 h / 20 °C View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
50361-53-0
→
反应条件
1914-65-4
1,2,3,4-四氢-1-萘甲酸
反应条件
hydrogenchloride; acetic acid; tin(ll) chloride Heating;
参考文献
Belletire, J. L.; Howard, H.; Donahue, K.
Synthetic Communications, 1982 , vol. 12, # 10 p. 763 - 770
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