5,8-二甲基-1-四酮合成路线 （共 25 条）
反应条件
1: 6.3 g / NaBH4 / ethanol / Ambient temperature
2: 4.38 g / POCl3 / 3 h / 100 °C
3: 3.2 g / AgNO3, NaOH / H2O / 4 h
View Scheme
参考文献
Reddy, P. Anantha; Rao, G. S. Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 9 p. 753 - 754
参考文献
Cocker et al.
Journal of the Chemical Society, 1953 , p. 2355,2359
反应条件
diethyl ether; bromine
Erwaermen des Reaktionsprodukts mit N,N-Diaethyl-anilin;
参考文献
Cocker et al.
Journal of the Chemical Society, 1953 , p. 2355,2359
反应条件
1: 90 percent / p-toluenesulfonic acid; 2,4-pentanediol / toluene / 48 h / Heating
2: m-chloroperbenzoic acid / CH2Cl2 / 6 h / 0 - 5 °C
3: 1.57 g / aq. H2SO4 / ethanol / 3 h / 60 °C
View Scheme
参考文献
Banerjee, Ajoy K.; Vera, William; Laya, Manuel S.
Synthetic Communications, 2004 , vol. 34, # 12 p. 2301 - 2308
反应条件
1: acetic anhydride / Heating
2: 7 percent / K-16 / 550 - 580 °C
3: 43 percent / sodium bichromate / acetic acid / Heating
View Scheme
参考文献
Prostakov, N. S.; Pleshakov, V. G.; Zainul Abedin, Md.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2462 - 2463
