2,2,2-三氯-1-(4,5-二氯-1H-吡咯-2-基)乙酮合成路线 (共 5 条)
反应条件
in methanol T=0 - 20°C; 13 h;
参考文献
Cheng, Ping; Clive, Derrick L.J.; Fernandopulle, Shimal; Chen, Zhenhua
Chemical Communications, 2013 , vol. 49, # 6 p. 558 - 560
反应条件
sulfuryl dichloride in chloroform
T=20°C; 26 h; Inert atmosphere; regioselective reaction;
参考文献
Guiheneuf, Solene; Paquin, Ludovic; Carreaux, Francois; Durieu, Emilie; Meijer, Laurent; Bazureau, Jean Pierre
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 5 p. 978 - 987
参考文献
Sterling Drug Inc.
Patent: US3963480 A1, 1976 ;
反应条件
sulfuryl dichloride in chloroform
T=20°C; Cooling with ice;
参考文献
Clark, Benjamin R.; O'Connor, Stephen; Fox, Deirdre; Leroy, Jacques; Murphy, Cormac D.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 18 p. 6306 - 6311
反应条件
sodium hydroxide in hexane; water
参考文献
Sterling Drug Inc.
Patent: US4046775 A1, 1977 ;