1-甲氧基-2-甲基-4-(甲硫基)苯合成路线 (共 9 条)
反应条件
potassium permanganate; potassium carbonate
参考文献
Shah; Bhatt; Kanga
Journal of the Chemical Society, 1933 , p. 1375,1379
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1934 , vol. 3/2, p. 155
反应条件
potassium hydroxide in methanol
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
反应条件
silver hexafluoroantimonate; antimony(V) pentachloride in 1,2-dichloro-ethane
3 h; Heating;
参考文献
Mukaiyama, Teruaki; Suzuki, Kaoru
Chemistry Letters, 1993 , # 1 p. 1 - 4
反应条件
1: 94 percent / Heating
2: KOH / methanol / 16 h / Heating
View Scheme
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
反应条件
1: 26 percent / ClSO2OH / diethyl ether / 12 h / Ambient temperature
2: 94 percent / Heating
3: KOH / methanol / 16 h / Heating
View Scheme
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
反应条件
potassium hydroxide in methanol
16 h; Heating;
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
参考文献
Shah; Bhatt; Kanga
Journal of the Chemical Society, 1933 , p. 1375,1379
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1934 , vol. 3/2, p. 155
反应条件
methanol; n-butyllithium
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884
反应条件
1: tin; aqueous HCl / zuletzt auf dem Dampfbad
2: aqueous NaOH
View Scheme
参考文献
Shah; Bhatt; Kanga
Journal of the Chemical Society, 1933 , p. 1375,1379
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1934 , vol. 3/2, p. 155