1: 92 percent / sulphuryl chloride / acetic acid / 3 h / Ambient temperature
2: 83 percent / Fremy's salt, K2HPO4 / H2O / 24 h / Ambient temperature
View Scheme
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
1: 83 percent / Br2 / acetic acid / 2 h
2: 96 percent / Fremy's salt, K2HPO4 / H2O / 3 h / Ambient temperature
View Scheme
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
1.1: K2CO3 / acetone
2.1: tetramethylene diamine; n-butyllithium / diethyl ether / 3 h / Heating
2.2: 97 percent / diethyl ether / 2 h / 20 °C
View Scheme
参考文献
Trost, Barry M.; Shen, Hong C.; Dong, Li; Surivet, Jean-Philippe; Sylvain, Catherine
Journal of the American Chemical Society, 2004 , vol. 126, # 38 p. 11966 - 11983