1: trans-2-buten-1-ol With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide; water T=20°C; Heck reaction; 0.25 h; 2: bromobenzene With 4'-hydroxyacetophenone oxime palladacycle catalyst in N,N-dimethyl acetamide; water T=120°C; Heck reaction; 10 h; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 17-18 p. 2572 - 2584
1: trans-2-buten-1-ol With α-cyclohexylcyclohexanemethanamine in water T=20°C; Heck reaction; 0.25 h; 2: iodobenzene With Kaiser oxime-derived complex on resin base in water T=120°C; Heck reaction; 10 h; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 17-18 p. 2572 - 2584
1: trans-2-buten-1-ol With caesium carbonate in water T=20°C; Heck reaction; 0.25 h; 2: iodobenzene With Kaiser oxime-derived complex on resin base in water T=120°C; Heck reaction; 14 h; Further stages. Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 17-18 p. 2572 - 2584
