in isopropyl alcohol
N2-atmosphere; addn. of 1 equiv. diol to 75percent soln. of Ti-complex (stirring), stirring at room temp. for 16 h; not isolated, reaction followed by NMR spectroscopy;
参考文献
Kemmitt, Tim; Daglish, Marc
Inorganic Chemistry, 1998 , vol. 37, # 8 p. 2063 - 2065
potassium carbonate in N,N-dimethyl-formamide
T=130°C; 12 h;
参考文献
Khalid, Naila; Khan, Muhammad Saif Ullah; Siddiqi, Humaira Masood; Akhter, Zareen; Iqbal, Naseer
Journal of the Chemical Society of Pakistan, 2011 , vol. 33, # 4 p. 570 - 577
1: With triethylamine in dichloromethane
T=20°C;
2: With sulfur trioxide pyridine complex; triethylamine in dichloromethane; dimethyl sulfoxide
T=20°C;
参考文献
Habrant, Damien; Stewart, Alan J.W.; Koskinen, Ari M.P.
Tetrahedron, 2009 , vol. 65, # 38 p. 7927 - 7934
