反应条件
in hexane
addn. of C3O2 to AlMe3 (1:5, hexane) under stirring at -78°C, warming to room temp., standing for 4 h; evapn. (vac.), distn. (vac.), diln. with hexane, cooling to -30°C and hydrolysing (NH4Cl-NH3-buffer, pH 8);
参考文献
Pandolfo, Luciano; Paiaro, Gastone; Vettori, Umberto
Gazzetta Chimica Italiana, 1989 , vol. 119, # 1 p. 59 - 62