1: 1,1-dimethylallyl alcohol With hydrogenchloride T=-5 - 0°C; 1.5 h; 2: With magnesium in tetrahydrofuran 5.3 h; 3: carbon dioxide 2 h; Title compound not separated from byproducts;
参考文献
Fekner, Tomasz; Mueller-Bunz, Helge; Guiry, Patrick J.
Organic Letters, 2006 , vol. 8, # 22 p. 5109 - 5112