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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
50400-51-6
合成路线
（共 7 条）
29976-75-8
6-甲基黄酮
→
反应条件
50400-51-6
反应条件
N-bromosuccinmide; dibenzoyl peroxide in benzene 6 h; Reflux;
参考文献
Roy, Somnath Singha; Chakraborty, Pramita; Bhattacharya, Sudin
European Journal of Medicinal Chemistry, 2014 , vol. 73, p. 195 - 209
98-88-4
苯甲酰氯
→
反应条件
50400-51-6
反应条件
1: potassium carbonate / acetone / 12 h / |Reflux 2: sodium acetate; acetic acid / 12 h / |Reflux 3: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
1450-72-2
2-羟基-5-甲基苯乙酮
→
反应条件
50400-51-6
反应条件
1: potassium carbonate / acetone / 12 h / |Reflux 2: sodium acetate; acetic acid / 12 h / |Reflux 3: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
29976-82-7
1-(2-羟基-5-甲基)-3-苯基-1,3-丙烷二酮
→
反应条件
50400-51-6
反应条件
1: sodium acetate; acetic acid / 12 h / |Reflux 2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
106-44-5
对甲酚
→
反应条件
50400-51-6
反应条件
1: sulfuric acid / 0.5 h / 20 °C 2: AlCl3, aluminium chloride / 2 h / 120 - 180 °C 3: potassium carbonate / acetone / 12 h / |Reflux 4: sodium acetate; acetic acid / 12 h / |Reflux 5: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
140-39-6
乙酸对甲酚酯
→
反应条件
50400-51-6
反应条件
1: AlCl3, aluminium chloride / 2 h / 120 - 180 °C 2: potassium carbonate / acetone / 12 h / |Reflux 3: sodium acetate; acetic acid / 12 h / |Reflux 4: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
4010-19-9
→
反应条件
50400-51-6
反应条件
1: potassium hydroxide / pyridine / 0.5 h / 100 °C 2: sulfuric acid / 0.5 h / 20 °C 3: N-bromosuccinmide; dibenzoyl peroxide / benzene / 6 h / |Reflux View Scheme
参考文献
Roy, Somnath Singha; Chakraborty, Pramita; Bhattacharya, Sudin
European Journal of Medicinal Chemistry, 2014 , vol. 73, p. 195 - 209
