Brownbridge, Peter; Hunt, Paul G.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1695 - 1706
1: 75 percent / NaH / tetrahydrofuran / 1.) 2 h, 2.) reflux, dark, 21 h
2: 99 percent / sodium borohydride / ethanol; H2O / 2 h / Ambient temperature
3: 93 percent / toluene-p-sulphonic acid monohydrate / benzene / 0.08 h / Heating; light excluded
View Scheme
参考文献
Fleming, Ian; Paterson, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 256 - 262
1: 75 percent / NaH / tetrahydrofuran / 1.) 2 h, 2.) reflux, dark, 21 h
2: 99 percent / sodium borohydride / ethanol; H2O / 2 h / Ambient temperature
3: 93 percent / toluene-p-sulphonic acid monohydrate / benzene / 0.08 h / Heating; light excluded
4: 98 percent / CCl4 / 6 h / Irradiation; sunlight
View Scheme
参考文献
Fleming, Ian; Paterson, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 256 - 262
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
1: 75 percent / NaH / tetrahydrofuran / 1.) 2 h, 2.) reflux, dark, 21 h
2: 99 percent / sodium borohydride / ethanol; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Fleming, Ian; Paterson, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 256 - 262
