2-(4-硝基苯基)乙酰氯合成路线 （共 63 条）
反应条件
1.1: LDA / tetrahydrofuran / 1 h / -78 °C 1.2: 78 percent / tetrahydrofuran / -78 - 20 °C View Scheme
参考文献
Katz, Christopher E.; Aube, Jeffrey
Journal of the American Chemical Society, 2003 , vol. 125, # 46 p. 13948 - 13949
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 4 h / |Inert atmosphere; |Cooling with ice 2: toluene-4-sulfonic acid / toluene View Scheme
参考文献
Zhang, Yu-Mo; Li, Minjie; Li, Wen; Huang, Zhiyuan; Zhu, Shaoyin; Yang, Bing; Wang, Xiao-Chun; Zhang, Sean Xiao-An
Journal of Materials Chemistry C, 2013 , vol. 1, # 34 p. 5309 - 5314
参考文献
Ward; Jenkins
Journal of Organic Chemistry, 1945 , vol. 10, p. 371
反应条件
1: lithium borohydride / tetrahydrofuran / 1 h / Ambient temperature 2: 69 percent / CBr4, Ph3P / benzene / 0.5 h / Ambient temperature View Scheme
参考文献
Herbert, Richard B.; Knaggs, Andrew R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 1 p. 109 - 114
反应条件
1: 17 percent / AlCl3 / CH2Cl2 / 0.33 h / 0 °C 2: 93 percent / LiAlH4 / tetrahydrofuran / 0.25 h / Ambient temperature 3: 1) thionyl chloride / 1) CH3CN, 0 deg C, 1 h, 2) CH3CN, room temperature, 1.5 h View Scheme
参考文献
Di Santo; Costi; Artico; Massa; Musiu; Scintu; Putzolu; La Colla
European Journal of Medicinal Chemistry, 1997 , vol. 32, # 2 p. 143 - 149
反应条件
aluminium trichloride 1) <30 deg C, 2) 50 deg C, 5 h;
参考文献
Meier, Herbert; Trickes, Georg; Laping, Elisabeth; Merkle, Ursula
Chemische Berichte, 1980 , vol. 113, # 1 p. 183 - 192
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 0 °C 2: sodium L-ascorbate; copper dichloride / water; acetonitrile / 20 - 80 °C 3: 2,9-dimethyl-1,10-phenanthroline; copper dichloride / acetonitrile / 20 h / 20 - 80 °C View Scheme
参考文献
Menendez, Christophe; Gau, Sylvain; Ladeira, Sonia; Lherbet, Christian; Baltas, Michel
European Journal of Organic Chemistry, 2012 , # 2 p. 409 - 416
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 0 °C 2: sodium L-ascorbate; copper dichloride / water; acetonitrile / 20 - 80 °C 3: 2,9-dimethyl-1,10-phenanthroline; copper dichloride / acetonitrile / 20 h / 20 - 80 °C View Scheme
参考文献
Menendez, Christophe; Gau, Sylvain; Ladeira, Sonia; Lherbet, Christian; Baltas, Michel
European Journal of Organic Chemistry, 2012 , # 2 p. 409 - 416
参考文献
Kipping,C. et al.
Journal fuer Praktische Chemie (Leipzig), 1973 , vol. 315, # 5 p. 887 - 894
参考文献
Kipping,C. et al.
Journal fuer Praktische Chemie (Leipzig), 1973 , vol. 315, # 5 p. 887 - 894
