N-(4-溴苯基)-N-甲基乙酰胺合成路线 （共 11 条）
反应条件
1: pyridine 2: aqueous HCl View Scheme
参考文献
Journal of the Chemical Society, , p. 3089,3092
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate / toluene / 12 h / 80 °C / |Inert atmosphere; |Schlenk technique 2: sodium acetate; hydroxylamine hydrochloride / methanol / 1 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Wang, Xi; Xu, Yan; Mo, Fanyang; Ji, Guojing; Qiu, Di; Feng, Jiajie; Ye, Yuxuan; Zhang, Songnan; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 28 p. 10330 - 10333
反应条件
1: N-(4-bromo-phenyl)-acetamide With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.5 h;
2: methyl iodide in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Meiji Seika Kaisha, Ltd.
Patent: EP1970377 A1, 2008 ;
Location in patent: Page/Page column 39 ;
反应条件
hexabromo-1,3-cyclopentadiene in acetonitrile
Heating;
参考文献
Fuchs, Benzion; Belsky, Yigal; Tartakovsky, Evgeny; Zizuashvili, Jakob; Weinman, Sarah
Journal of the Chemical Society, Chemical Communications, 1982 , # 14 p. 778 - 779
反应条件
pyridine; tert.-butylhydroperoxide; iron(II) chloride in acetonitrile
T=85°C; 2 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Ma, Lina; Jia, Fan; Li, Zhiping
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5638 - 5646
反应条件
iron(II) chloride in acetonitrile
T=85°C; 2 h; Inert atmosphere;
参考文献
Li, Yuanming; Ma, Lina; Jia, Fan; Li, Zhiping
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5638 - 5646
反应条件
1: pyridine / CH2Cl2
2: NaH / tetrahydrofuran / 20 °C
View Scheme
参考文献
Yamasaki, Ryu; Tanatani, Aya; Azumaya, Isao; Saito, Shoichi; Yamaguchi, Kentaro; Kagechika, Hiroyuki
Organic Letters, 2003 , vol. 5, # 8 p. 1265 - 1267
反应条件
1: hydrochloric acid; H2O; sodium nitrite
View Scheme
参考文献
Wurster; Scheibe
Chemische Berichte, 1879 , vol. 12, p. 1819
反应条件
1: tin; hydrochloric acid
View Scheme
参考文献
Wurster; Scheibe
Chemische Berichte, 1879 , vol. 12, p. 1819
参考文献
Wurster; Scheibe
Chemische Berichte, 1879 , vol. 12, p. 1819
