1-(4-溴苯基)-1H-吡咯合成路线 （共 9 条）
反应条件
iron(III) chloride heptahydrate in water T=60°C; Paal-Knorr pyrrole synthesis;
参考文献
Azizi, Najmedin; Khajeh-Amiri, Alireza; Ghafuri, Hossein; Bolourtchian, Mohammad; Saidi, Mohammad Reza
Synlett, 2009 , # 14 p. 2245 - 2248
反应条件
sodium hydroxide; copper(l) iodide; tetrabutylammomium bromide in toluene 22 h; Heating;
参考文献
Chang, Joyce Wei Wei; Xu, Xiuhui; Chan, Philip Wai Hong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 245 - 248
反应条件
MgI2 etherate in acetonitrile T=80°C; Clauson-Kaas pyrrole synthesis; chemoselective reaction;
参考文献
Zhang, Xingxian; Shi, Junchen
Tetrahedron, 2011 , vol. 67, # 5 p. 898 - 903
反应条件
MgI2 etherate in acetonitrile T=80°C; Clauson-Kaas pyrrole synthesis; chemoselective reaction;
参考文献
Zhang, Xingxian; Shi, Junchen
Tetrahedron, 2011 , vol. 67, # 5 p. 898 - 903
反应条件
Grubb's 2nd generation catalyst; CuCl2·2H2O; oxygen in 1,2-dichloro-ethane T=60°C; 24 h;
参考文献
Chen, Weiqiang; Wang, Jianhui
Organometallics, 2013 , vol. 32, # 6 p. 1958 - 1963
反应条件
1: hydrogenchloride; indium / water / 0.17 h / 20 °C 2: water / 1.08 h / 20 °C View Scheme
参考文献
Das, Biswanath; Shinde, Digambar Balaji; Kanth, Boddu Shashi; Kumar, Jayprakash Narayan
Synthetic Communications, 2012 , vol. 42, # 4 p. 548 - 553
反应条件
1.54H2O*Cl2Ni; ICy*HBF4 in tetrahydrofuran T=-10°C; Kumada coupling reaction; 1.5 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 22 p. 8478 - 8481
反应条件
1: 1-(para-bromophenyl)-1H-pyrrole With 2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran T=-75°C; 1 h; 2: carbon dioxide in tetrahydrofuran; diethyl ether T=20°C; Further stages.;
参考文献
Fogassy, Katalin; Kovacs, Krisztina; Keseru, Gyoergy M.; Toke, Laszlo; Faigl, Ferenc
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1039 - 1043
反应条件
1: 1-(para-bromophenyl)-1H-pyrrole With n-butyllithium in tetrahydrofuran; hexane T=-70°C; 2 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-70 - 20°C; 4 h;
参考文献
Nakazaki, Jotaro; Chung, InGwon; Matsushita, Michio M.; Sugawara, Tadashi; Watanabe, Ryoji; Izuoka, Akira; Kawada, Yuzo
Journal of Materials Chemistry, 2003 , vol. 13, # 5 p. 1011 - 1022
