反应条件
lithium aluminium tetrahydride; dihydrogen peroxide
1.) THF, reflux, 15 h, 2.) THF, water, rt, 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cristau, Henri-Jean; Labaudiniere, Lydie; Christol, Henri
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 15, p. 359 - 372
