1,3,5-三(4-羧基苯基)苯合成路线 (共 15 条)
反应条件
T=125°C; 72 h; Title compound not separated from byproducts.;
参考文献
Njus, Jeffrey M.; Sandman, Daniel J.; Yang, Lin; Foxman, Bruce M.
Macromolecules, 2005 , vol. 38, # 18 p. 7645 - 7652
反应条件
1: 41 percent / triethyl orthoformate 2: 60 percent / 1.6 M n-BuLi / tetrahydrofuran; hexane / -60 °C View Scheme
参考文献
JX Nippon Oil and Energy Corporation; WATANABE Daisuke; OSHIMA Shinji; RUDY Coquet; KITAGAWA Susumu
Patent: EP2586766 A1, 2013 ;
反应条件
1: AlCl3 / 210 °C 2: aq. HNO3 / 170 °C View Scheme
参考文献
Claus
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2> 41, p. 414
Journal fuer Praktische Chemie (Leipzig), 1893 , vol. <2> 47, p. 420
反应条件
1: para-bromoacetophenone 2: With n-butyllithium 3: carbon dioxide
参考文献
Zhang, Zhenxin; Zhao, Wei; Ma, Baochun; Ding, Yong
Catalysis Communications, 2010 , vol. 12, # 4 p. 318 - 322
反应条件
water; sodium hydroxide
参考文献
Ibarra, Ilich A.; Lin, Xiang; Yang, Sihai; Blake, Alexander J.; Walker, Gavin S.; Barnett, Sarah A.; Allan, David R.; Champness, Neil R.; Hubberstey, Peter; Schroeder, Martin
Chemistry - A European Journal, 2010 , vol. 16, # 46 p. 13671 - 13679