6,6-二甲基十一烷-2,5,10-三酮合成路线 （共 14 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol
3 h;
参考文献
Bischofberger, Norbert; Weck, Guy de; Frei, Bruno; Wolf, Hans Richard; Jeger, Oskar
Helvetica Chimica Acta, 1981 , vol. 64, # 6 p. 1766 - 1776
反应条件
hydrogen; palladium on activated charcoal in ethanol
12 h; Yield given;
参考文献
O'Sullivan, Anthony; Frei, Bruno; Jeger, Oskar
Helvetica Chimica Acta, 1986 , vol. 69, p. 555 - 559
反应条件
air; cation radical salt of tris(4-bromophenyl)aminium hexachloroantimonate in dichloromethane
Ambient temperaturefurther reagent ((o,p-Br2C6H3)3N*+*SbCl6);
参考文献
Lopez, Luigi; Mele, Giuseppe; Mazzeo, Costanza
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 7 p. 779 - 782
反应条件
1: 14 percent / CoTPP / diethyl ether; CHCl3 / 0.25 h / Heating
2: 98 percent / H2 / Pd-C / ethanol / 3 h
View Scheme
参考文献
Bischofberger, Norbert; Weck, Guy de; Frei, Bruno; Wolf, Hans Richard; Jeger, Oskar
Helvetica Chimica Acta, 1981 , vol. 64, # 6 p. 1766 - 1776
反应条件
1: 73 percent / O2, Rose Bengal / methanol / 48 h / Irradiation
2: 14 percent / CoTPP / diethyl ether; CHCl3 / 0.25 h / Heating
3: 98 percent / H2 / Pd-C / ethanol / 3 h
View Scheme
参考文献
Bischofberger, Norbert; Weck, Guy de; Frei, Bruno; Wolf, Hans Richard; Jeger, Oskar
Helvetica Chimica Acta, 1981 , vol. 64, # 6 p. 1766 - 1776
反应条件
hydrogen; palladium in ethanol
参考文献
Ehrenfreund,J. et al.
Helvetica Chimica Acta, 1974 , vol. 57, p. 2704 - 2707
反应条件
1: aq. TsOH / diethyl ether
2: H2 / Pd / ethanol
View Scheme
参考文献
Ehrenfreund,J. et al.
Helvetica Chimica Acta, 1974 , vol. 57, p. 2704 - 2707
反应条件
hematoporphyrin IX in dichloromethane
Irradiation;
参考文献
Skorianetz,W.; Ohloff,G.
Helvetica Chimica Acta, 1973 , vol. 56, p. 2151 - 2166
反应条件
in pentane
Irradiation;
参考文献
von Wartburg,B.R. et al.
Helvetica Chimica Acta, 1973 , vol. 56, # 6 p. 1948 - 1955
参考文献
Mischne, Mirta
Tetrahedron Letters, 2003 , vol. 44, # 31 p. 5823 - 5826
