甘菊环-2-胺; 环戊并环庚五烯-2-胺; 薁-2-胺合成路线 （共 7 条）
反应条件
trifuran-2-yl-phosphane; tetraethylammonium iodide; zinc; NiCl2((PPh3)P)2 in tetrahydrofuran
T=50°C; 12 h;
参考文献
Kurotobi, Kei; Tabata, Hiroshi; Miyauchi, Masato; Murafuji, Toshihiro; Sugihara, Yoshikazu
Synthesis, 2002 , # 8 p. 1013 - 1016
反应条件
hydrazine hydrate in tetrahydrofuran
T=20°C; 24 h;
参考文献
Fujinaga, Masayuki; Suetake, Kouichi; Gyoji, Kazuhiro; Murafuji, Toshihiro; Kurotobi, Kei; Sugihara, Yoshikazu
Synthesis, 2008 , # 23 art. no. F14108SS, p. 3745 - 3748
反应条件
ethanolic alkali
Hydrolysis.und anschliessenden Decarboxylierung;
参考文献
Nozoe et al.
Chemistry and Industry (London, United Kingdom), 1955 , p. 1257
反应条件
in pyridine
T=125 - 130°C;
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, # 7 p. 1179 - 1188
反应条件
1: NaOEt / ethanol
2: aq. KOH / ethanol / Heating
3: pyridine / 125 - 130 °C
View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, # 7 p. 1179 - 1188
反应条件
1: NaOEt / ethanol
2: aq. KOH / ethanol / Heating
3: pyridine / 125 - 130 °C
View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, # 7 p. 1179 - 1188
反应条件
1: NaOEt / ethanol
2: aq. KOH / ethanol / Heating
3: pyridine / 125 - 130 °C
View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, # 7 p. 1179 - 1188
