3-苯基-1,2,4-噻二唑-5-甲酸乙酯合成路线 (共 7 条)
反应条件
in para-xylene
T=160°C; 0.166667 h; Microwave irradiation;
参考文献
Fordyce, Euan A.F.; Morrison, Angus J.; Sharp, Robert D.; Paton, R. Michael
Tetrahedron, 2010 , vol. 66, # 35 p. 7192 - 7197
反应条件
in 1,3,5-trimethyl-benzene
T=161°C; 26 h; Heating;
参考文献
Paton, R. Michael; Robertson, Fiona M.; Ross, John F.; Crosby, John
Journal of the Chemical Society, Chemical Communications, 1980 , # 15 p. 714 - 715
反应条件
1: chlorobenzene
2: aq. EtOH
View Scheme
参考文献
Franz,J.E. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 620 - 626
参考文献
Franz,J.E. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 620 - 626
反应条件
in decalin
Inert atmosphere;
参考文献
Porcal, Williams; Hernandez, Paola; Gonzalez, Mercedes; Ferreira, Ana; Olea-Azar, Claudio; Cerecetto, Hugo; Castro, Ana
Journal of Medicinal Chemistry, 2008 , vol. 51, # 19 p. 6150 - 6159
反应条件
in acetonitrile
3.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Pavlik, James W.; Changtong, Chuchawin; Vikki
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4855 - 4861
反应条件
in acetonitrile
5 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Pavlik, James W.; Changtong, Chuchawin; Vikki
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4855 - 4861