N,N-二甲基环戊烷甲酰胺合成路线 （共 6 条）
反应条件
1: LiAlH4; diethyl ether View Scheme
参考文献
Cope et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 4720,4727
反应条件
1: LiAlH4; diethyl ether 2: methanol; aqueous hydrogen peroxide / Erhitzen des Reaktionsprodukts unter vermindertem Druck View Scheme
参考文献
Journal of the American Chemical Society, , vol. 79, p. 4720,4727
反应条件
pyridine; hydrogenchloride in dichloromethane
4 h;
参考文献
Tromm, Peter; Heimgartner, Heinz
Helvetica Chimica Acta, 1988 , vol. 71, p. 2071 - 2084
反应条件
lithium diethylamide in tetrahydrofuran
T=-30 - 20°C;
参考文献
Cuvigny,T. et al.
Canadian Journal of Chemistry, 1979 , vol. 57, p. 1201 - 1205
反应条件
1: 88.5 percent / SOCl2 / 3 h / Heating
2: 93 percent / 1) pyridine; 2) 1 N HCl / CH2Cl2 / 4 h
View Scheme
参考文献
Tromm, Peter; Heimgartner, Heinz
Helvetica Chimica Acta, 1988 , vol. 71, p. 2071 - 2084
参考文献
Mousseron et al.
Bulletin de la Societe Chimique de France, 1952 , p. 767,775
