反应条件
1.1: sulfuric acid / Heating
2.1: LiAlH4 / diethyl ether / 0 °C
3.1: HBr / benzene / Heating
4.1: pyridinium p-toluenesulfonate / CH2Cl2 / 24 h / 20 °C
5.1: magnesium / tetrahydrofuran / 3 h / 55 °C
5.2: dilithium tetrachlorocuprate(II) / tetrahydrofuran / 3 h / 0 °C
6.1: 4.5 g / pyridinium p-toluenesulfonate / methanol / 3 h / Heating
View Scheme
参考文献
Drescher, Simon; Meister, Annette; Blume, Alfred; Karlsson, Goeran; Almgren, Mats; Dobner, Bodo
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5300 - 5307