(1H-吡咯-2-基)乙腈合成路线 （共 12 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Herz
Journal of the American Chemical Society, 1953 , vol. 75, p. 483
反应条件
methanol; ammonia; platinum Hydrogenation;
参考文献
Herz; Tocker
Journal of the American Chemical Society, 1955 , vol. 77, p. 6353
反应条件
potassium hydroxide in methanol; water 1.5 h; Heating;
参考文献
Janda, Miroslav; Srogl, Jan; Holy, Petr; Jakoubkova, Marie
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 10 p. 2404 - 2409
反应条件
tetrabutylammomium bromide; sodium thiosulfate; methyloxirane in various solvent(s)
T=40°C; Substitution; Photolysis;
参考文献
Byers, Jeffrey H.; Campbell, John E.; Knapp, Faith H.; Thissell, Jameson G.
Tetrahedron Letters, 1999 , vol. 40, # 14 p. 2677 - 2680
反应条件
sodium chloride; triethylamine in dichloromethane; water
参考文献
Syntex (U.S.A.) Inc.
Patent: US4410534 A1, 1983 ;
反应条件
toluene-4-sulfonic acid in water; N,N-dimethyl-formamide
T=115°C; 48 h;
参考文献
Muchowski, Joseph M.; Scheller, Marcus E.
Synthetic Communications, 1987 , vol. 17, # 7 p. 863 - 876
反应条件
methyl iodide
Erwaermen des entstandenen Methojodids mit NaCN und H2O;
参考文献
Herz; Tocker
Journal of the American Chemical Society, 1955 , vol. 77, p. 6353
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Herz
Journal of the American Chemical Society, 1953 , vol. 75, p. 483
反应条件
in N,N-dimethyl-formamide
2 h;
参考文献
Janda, Miroslav; Srogl, Jan; Holy, Petr; Jakoubkova, Marie
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 10 p. 2404 - 2409
反应条件
1: meta-chloroperbenzoic acid, K2CO3 / -23 °C
2: 1) 65 deg C, 6 h or 110 deg C, 1 h
View Scheme
参考文献
Barcock; Moorcroft; Storr; Young; Fuller
Tetrahedron Letters, 1993 , vol. 34, # 7 p. 1187 - 1190
反应条件
pyridine; 18-crown-6 ether; NOBF4
1) CH2Cl2, -78 deg C, 45 min; Yield given. Multistep reaction;
参考文献
Loeppky; Outram; Tomasik; Faulconer
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4271 - 4274
