N-(2-甲氧基乙基)-2,6-二甲苯胺合成路线 （共 7 条）
反应条件
palladium on charcoal in toluene
参考文献
Ciba-Geigy Corporation
Patent: US4188341 A1, 1980 ;
反应条件
palladium on charcoal in 1,4-dioxane
参考文献
Ciba-Geigy Corporation
Patent: US4188341 A1, 1980 ;
反应条件
1: 96.5 percent / 10percent aq.NaOH / toluene / 1.17 h / 25 °C
2: 95.7 percent / 25percent methanolic NaOCH3 / methanol / 5 h / Ambient temperature
3: 2.) 6M HCl / 1.) methanol, 83 deg C, 6 h, 2.) 30 min, reflux
View Scheme
参考文献
Fancher, L.W.; Gless, R.D.; Wong, R.Y.
Tetrahedron Letters, 1988 , vol. 29, # 40 p. 5095 - 5098
反应条件
trimethylamine in methanol; benzene
参考文献
Ciba-Geigy Corporation
Patent: US4283221 A1, 1981 ;
反应条件
hydrogenchloride; sodium hydrogencarbonate in water
参考文献
Ciba-Geigy Corporation
Patent: US4188341 A1, 1980 ;
反应条件
1: 95.7 percent / 25percent methanolic NaOCH3 / methanol / 5 h / Ambient temperature
2: 2.) 6M HCl / 1.) methanol, 83 deg C, 6 h, 2.) 30 min, reflux
View Scheme
参考文献
Fancher, L.W.; Gless, R.D.; Wong, R.Y.
Tetrahedron Letters, 1988 , vol. 29, # 40 p. 5095 - 5098
反应条件
hydrogenchloride
1.) methanol, 83 deg C, 6 h, 2.) 30 min, reflux; Yield given. Multistep reaction;
参考文献
Fancher, L.W.; Gless, R.D.; Wong, R.Y.
Tetrahedron Letters, 1988 , vol. 29, # 40 p. 5095 - 5098
