2,3,7,8-四溴二苯并对二噁英合成路线 （共 4 条）
反应条件
bromine in trifluoroacetic acid
6 h; Heating;
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.
Russian Journal of General Chemistry, 1993 , vol. 63, # 8.2. p. 1279 - 1286
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 8 p. 1831 - 1842
反应条件
1: 1.) Na, hexamethylphosphoramide / 1.) 100-150 deg C, 2.) 200-210 deg C, 3 h
2: 97 percent / Br2, CF3COOH / 6 h / Heating
View Scheme
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.; Rembovskii, V. R.; Troshkin, N. M.; Baulin, S. I.
Doklady Chemistry, 1993 , vol. 332, # 4 p. 225 - 229
Dokl. Akad. Nauk SSSR Ser. Khim., 1993 , vol. 332, # 4 p. 461 - 465
反应条件
1: 1.) Na, hexamethylphosphoramide / 1.) 100-150 deg C, 2.) 200-210 deg C, 3 h
2: 97 percent / Br2, CF3COOH / 6 h / Heating
View Scheme
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.; Rembovskii, V. R.; Troshkin, N. M.; Baulin, S. I.
Doklady Chemistry, 1993 , vol. 332, # 4 p. 225 - 229
Dokl. Akad. Nauk SSSR Ser. Khim., 1993 , vol. 332, # 4 p. 461 - 465
反应条件
T=400°C; thermolysis; Further byproducts given;
参考文献
Bieniek, Dieter; Bahadir, Muefit; Korte, Friedhelm
Heterocycles, 1989 , vol. 28, # 2 p. 719 - 722
