1-苄基-3-哌啶甲酸甲酯合成路线 (共 5 条)
反应条件
1: tetrahydrofuran / 16 h / 66 °C 2: 98 percent / H2, Na2CO3 / 10percent Pd/C / ethanol / 2280 Torr 3: 99 percent / Lawesson's reagent / tetrahydrofuran 5: 1.) PrMgBr, 2.) NaBH4 View Scheme
参考文献
Cook, Gregory R.; Beholz, Lars G.; Stille, John R.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3575 - 3584
反应条件
1: 98 percent / H2, Na2CO3 / 10percent Pd/C / ethanol / 2280 Torr 2: 99 percent / Lawesson's reagent / tetrahydrofuran 4: 1.) PrMgBr, 2.) NaBH4 View Scheme
参考文献
Cook, Gregory R.; Beholz, Lars G.; Stille, John R.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3575 - 3584
反应条件
1: diethyl ether / 12 h / Ambient temperature 2: tetrahydrofuran / 16 h / 66 °C 3: 98 percent / H2, Na2CO3 / 10percent Pd/C / ethanol / 2280 Torr 4: 99 percent / Lawesson's reagent / tetrahydrofuran 6: 1.) PrMgBr, 2.) NaBH4 View Scheme
参考文献
Cook, Gregory R.; Beholz, Lars G.; Stille, John R.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3575 - 3584
反应条件
1: 99 percent / Lawesson's reagent / tetrahydrofuran 3: 1.) PrMgBr, 2.) NaBH4 View Scheme
参考文献
Cook, Gregory R.; Beholz, Lars G.; Stille, John R.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3575 - 3584
反应条件
2: 1.) PrMgBr, 2.) NaBH4 View Scheme
参考文献
Cook, Gregory R.; Beholz, Lars G.; Stille, John R.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3575 - 3584