2-甲基-6-氨基-2H-吲唑合成路线 (共 5 条)
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; 12 h;
参考文献
Qi, Haofei; Chen, Ligong; Liu, Bingni; Wang, Xinran; Long, Li; Liu, Dengke
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 4 p. 1108 - 1110
反应条件
1: With potassium hydroxide; water T=75°C; 0.5 h; 2: With hydrogen; palladium on activated charcoal in methanol; dichloromethane T=50°C; P=2250.23 Torr; Further stages.;
参考文献
Miloudi, Abdellah; El Abed, Douniazed; Boyer, Gerard; Galy, Jean-Pierre
Heterocycles, 2006 , vol. 68, # 12 p. 2595 - 2605
反应条件
1: 43 percent / KOH; water / 0.5 h / 75 °C 2: 42 percent / conc. HCl; SnCl2*H2O / methanol / Heating View Scheme
参考文献
Boyer, Gerard; Galy, Jean-Pierre; Faure, Robert; Elguero, Jose; Barbe, Jacques
Journal of Chemical Research, Miniprint, 1990 , # 11 p. 2601 - 2615
反应条件
hydrogenchloride; tin(ll) chloride in methanol Heating;
参考文献
Miloudi, Abdellah; El Abed, Douniazed; Boyer, Gerard; Galy, Jean-Pierre
Heterocycles, 2006 , vol. 68, # 12 p. 2595 - 2605
反应条件
sulfuric acid; boric acid; sodium nitrite in water
boiling 10 min.;
参考文献
Stankyavichyus, A. P.; Terent'ev, P. B.; Bolotin, V. A.; Lashin, V. V.; Rakhimi, I. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , p. 403 - 409
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , vol. 24, # 4 p. 491 - 498