3,4,5-三氯三氟甲苯合成路线 (共 21 条)
反应条件
sodium nitrite; Copper(I)chloride in hydrogenchloride; water
参考文献
Rohm and Haas Company
Patent: US31455 E1, 1983 ;
反应条件
sodium nitrite; Copper(I)chloride in hydrogenchloride; water
参考文献
Imperial Chemical Industries Limited
Patent: US4384135 A1, 1983 ;
反应条件
hydrogenchloride; sodium nitrite; Copper(I)chloride in dichloromethane; water
参考文献
Imperial Chemical Industries Limited
Patent: US4384135 A1, 1983 ;
反应条件
sulfuric acid; chlorine; AlCl3, aluminium chloride; iron T=110°C; Product distribution / selectivity;
参考文献
Zhejiang Weihua Chemical Co., Ltd.
Patent: US2009/240083 A1, 2009 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride T=5 - 120°C; P=15001.5 Torr; 2 h; Product distribution / selectivity;
参考文献
FINCHIMICA S.p.A.
Patent: EP1528052 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
chlorine; iron(III) chloride T=80°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ushakov, A. A.; Alikhanov, P. P.; Motsarev, G. V.; Kalinachenko, V. R.; Kuznetsova, G. N.; Kolbasov, V. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1993 - 1996
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2187 - 2191
反应条件
chlorine; iron(III) chloride
参考文献
Ushakov,A.A. et al.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 2140 - 2144
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 10 p. 2204 - 2209
反应条件
chlorine; iron(III) chloride T=80°C; other products; Product distribution;
参考文献
Alikhanov, P. P.; Ushakov, A. A.; Kuznetsova, G. N.; Kalinachenko, V. R.; Motsarev, G. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 734 - 740
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 809 - 817
反应条件
chlorine; iron(III) chloride T=80°C; Product distribution;
参考文献
Alikhanov, P. P.; Ushakov, A. A.; Kuznetsova, G. N.; Kalinachenko, V. R.; Motsarev, G. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 734 - 740
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 809 - 817
反应条件
chlorine; iron(III) chloride T=80°C; other time; Product distribution;
参考文献
Ushakov, A. A.; Alikhanov, P. P.; Motsarev, G. V.; Kalinachenko, V. R.; Kuznetsova, G. N.; Kolbasov, V. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1993 - 1996
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2187 - 2191