3,4,5-三氯三氟甲苯合成路线 （共 21 条）
反应条件
potassium fluoride; nitrobenzene; (N,N'-dimethylimidazolidino)tetramethylguanidinium chloride in sulfolane T=200 - 220°C; P=6750.68 Torr; 17 h;
参考文献
Pleschke, Axel; Marhold, Albrecht
Patent: US2006/9643 A1, 2006 ;
Location in patent: Page/Page column 5 ;
反应条件
monomethyldichlorosilane T=240°C; (electron irradiation);
参考文献
Vaks,E.A.; Vainshtein,B.I.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, # 4 p. 782 - 785,713 - 716
反应条件
1-methyl-pyrrolidin-2-one; ammonia T=0 - 190°C; 8 h;
参考文献
FINCHIMICA S.p.A.
Patent: EP1528052 A1, 2005 ;
Location in patent: Page/Page column 6-7 ;
反应条件
1-methyl-pyrrolidin-2-one; ammonia T=0 - 190°C; 8 h;
参考文献
FINCHIMICA S.p.A.
Patent: EP1528052 A1, 2005 ;
Location in patent: Page/Page column 7 ;
反应条件
hydrazine in tetrahydrofuran T=50°C; 24 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: WO2008/113661 A2, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
potassium fluoride; tetra-phenylphosphonium bromide in sulfolane T=100 - 190°C; P=75.0075 Torr; 15 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: WO2008/113660 A1, 2008 ;
Location in patent: Page/Page column 11 ;
反应条件
tetraphenylphosphonium hydrogendifluoride 2 h; Heating;
参考文献
Brown, S. J.; Clark, J. H.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 251 - 258
反应条件
tetraphenylphosphonium hydrogendifluoride 2 h; Heating;
参考文献
Brown, S. J.; Clark, J. H.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 251 - 258
反应条件
chlorine; iron(III) chloride
T=80°C; Yield given;
参考文献
Ushakov, A. A.; Alikhanov, P. P.; Motsarev, G. V.; Kalinachenko, V. R.; Kuznetsova, G. N.; Kolbasov, V. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1993 - 1996
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2187 - 2191
反应条件
in sulfolane; hexane
参考文献
Rohm and Haas Company
Patent: US4419122 A1, 1983 ;
