1: With chloro-trimethyl-silane in tetrahydrofuran
T=0°C; 4 h; Inert atmosphere;
2: With hydrogenchloride; water in tetrahydrofuran
T=20°C; 3 h; Inert atmosphere;
tetrabutylammomium bromide; Sm(III) chloride in N,N-dimethyl-formamide
T=20°C; 6 h; Electrochemical reaction; Product distribution; Further Variations:Catalysts;
参考文献
Batsanov, Andrei S.; Bruce, James I.; Ganesh, Thota; Low, Paul J.; Kataky, Ritu; Puschmann, Horst; Steel, Patrick G.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 7 p. 932 - 937