4-(二甲基氨基)-2-苯基丁腈合成路线 （共 18 条）
反应条件
sodium amide; benzene
参考文献
Klosa
Archiv der Pharmazie (Weinheim, Germany), 1953 , vol. 286, p. 108,110
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Wilson
Journal of the Chemical Society, 1952 , p. 6,8
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; oxygen in dimethyl sulfoxide 3 h;
参考文献
Donetti, Arturo; Boniardi, Orazio; Ezhaya, Antoine
Synthesis, 1980 , # 12 p. 1009 - 1011
反应条件
η5-cyclopentadienyl-η4-cycloocta-1,5-diene-cobalt(I) in toluene T=140°C; P=10640 Torr; 36 h;
参考文献
Botteghi, Carlo; Chelucci, Giorgio; Ponte, Gino Del; Marchetti, Mauro; Paganelli, Stefano
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7125 - 7127
反应条件
1: NaNH2; toluene / anschliessendes Behandeln mit 1-Brom-2-chlor-aethan 2: palladium; aqueous ethanol / Hydrogenation View Scheme
参考文献
Kaegi; Miescher
Helvetica Chimica Acta, 1949 , vol. 32, p. 2489,2497
参考文献
Klosa
Archiv der Pharmazie (Weinheim, Germany), 1953 , vol. 286, p. 108,110
反应条件
carbon disulfide; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane
0.5 h; Ambient temperature;
参考文献
Botteghi, Carlo; Chelucci, Giorgio; Ponte, Gino Del; Marchetti, Mauro; Paganelli, Stefano
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7125 - 7127
反应条件
sodium amide; toluene
参考文献
Clarke; Mooradian
Journal of the American Chemical Society, 1949 , vol. 71, p. 2825
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Kwartler; Lucas
Journal of the American Chemical Society, 1946 , vol. 68, p. 2395
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Kaegi; Miescher
Helvetica Chimica Acta, 1949 , vol. 32, p. 2489,2497
反应条件
1: H2 / HRh(CO)(PPh3)3 / benzene / 24 h / 80 °C / 76000 Torr
2: NH2OH
3: 95 percent / CS2, n-Bu4N(1+)*HSO4(1-), 15percent aq. NaOH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Botteghi, Carlo; Chelucci, Giorgio; Ponte, Gino Del; Marchetti, Mauro; Paganelli, Stefano
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7125 - 7127
反应条件
1: NH2OH
2: 95 percent / CS2, n-Bu4N(1+)*HSO4(1-), 15percent aq. NaOH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Botteghi, Carlo; Chelucci, Giorgio; Ponte, Gino Del; Marchetti, Mauro; Paganelli, Stefano
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7125 - 7127
参考文献
Anker; Cook
Journal of the Chemical Society, 1948 , p. 806,808
