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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
二十八酸
合成路线
（共 20 条）
96374-71-9
→
反应条件
506-48-9
二十八酸
反应条件
sodium hydroxide; hydrazine hydrate; ethylene glycol T=220°C;
参考文献
Breusch et al.
Fette und Seifen, 1959 , vol. 61, p. 891
557-61-9
二十八烷醇
→
反应条件
506-48-9
二十八酸
反应条件
chromium; acetic acid
参考文献
Zhang, Hong-Yan; Yamakawa, Yu-Ichiro; Matsuya, Yuji; Toyooka, Naoki; Tohda, Chihiro; Awale, Suresh; Li, Feng; Kadota, Shigetoshi; Tezuka, Yasuhiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 604 - 608
103165-11-3
→
反应条件
506-48-9
二十八酸
反应条件
sodium; hydrazine hydrate; ethylene glycol T=200°C;
参考文献
Lukes; Dolezal
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 1100,1102,1107
119696-25-2
→
反应条件
506-48-9
二十八酸
反应条件
sodium hydroxide; hydrazine hydrate in ethylene glycol
参考文献
Watanabe,A.
Bulletin of the Chemical Society of Japan, 1961 , vol. 34, p. 398 - 402
52363-35-6
→
反应条件
506-48-9
二十八酸
反应条件
potassium hydroxide in ethanol
参考文献
Kondo; Takemoto
Chemical and Pharmaceutical Bulletin, 1973 , vol. 21, # 10 p. 2265 - 2267
1611-56-9
11-溴-1-十一醇
→
反应条件
506-48-9
二十八酸
反应条件
1: triethylamine / dichloromethane 2: n-butyllithium; N,N,N',N',N'',N''-hexamethylphosphoric triamide / tetrahydrofuran 3: hydrogen; palladium 10 on activated carbon / ethyl acetate 4: pyridinium chlorochromate / dichloromethane 5: sodium hexamethyldisilazane / tetrahydrofuran 6: tetrabutyl ammonium fluoride / tetrahydrofuran 7: hydrogen; palladium 10 on activated carbon / ethyl acetate View Scheme
参考文献
Zhang, Hong-Yan; Yamakawa, Yu-Ichiro; Matsuya, Yuji; Toyooka, Naoki; Tohda, Chihiro; Awale, Suresh; Li, Feng; Kadota, Shigetoshi; Tezuka, Yasuhiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 604 - 608
172995-51-6
→
反应条件
506-48-9
二十八酸
反应条件
1: n-butyllithium; N,N,N',N',N'',N''-hexamethylphosphoric triamide / tetrahydrofuran 2: hydrogen; palladium 10 on activated carbon / ethyl acetate 3: pyridinium chlorochromate / dichloromethane 4: sodium hexamethyldisilazane / tetrahydrofuran 5: tetrabutyl ammonium fluoride / tetrahydrofuran 6: hydrogen; palladium 10 on activated carbon / ethyl acetate View Scheme
参考文献
Zhang, Hong-Yan; Yamakawa, Yu-Ichiro; Matsuya, Yuji; Toyooka, Naoki; Tohda, Chihiro; Awale, Suresh; Li, Feng; Kadota, Shigetoshi; Tezuka, Yasuhiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 604 - 608
1538660-98-8
→
反应条件
506-48-9
二十八酸
反应条件
1: hydrogen; palladium 10 on activated carbon / ethyl acetate 2: pyridinium chlorochromate / dichloromethane 3: sodium hexamethyldisilazane / tetrahydrofuran 4: tetrabutyl ammonium fluoride / tetrahydrofuran 5: hydrogen; palladium 10 on activated carbon / ethyl acetate View Scheme
参考文献
Zhang, Hong-Yan; Yamakawa, Yu-Ichiro; Matsuya, Yuji; Toyooka, Naoki; Tohda, Chihiro; Awale, Suresh; Li, Feng; Kadota, Shigetoshi; Tezuka, Yasuhiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 604 - 608
236754-35-1
→
反应条件
506-48-9
二十八酸
反应条件
1: pyridinium chlorochromate / dichloromethane 2: sodium hexamethyldisilazane / tetrahydrofuran 3: tetrabutyl ammonium fluoride / tetrahydrofuran 4: hydrogen; palladium 10 on activated carbon / ethyl acetate View Scheme
参考文献
Zhang, Hong-Yan; Yamakawa, Yu-Ichiro; Matsuya, Yuji; Toyooka, Naoki; Tohda, Chihiro; Awale, Suresh; Li, Feng; Kadota, Shigetoshi; Tezuka, Yasuhiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 604 - 608
1538660-99-9
→
反应条件
506-48-9
二十八酸
反应条件
1: sodium hexamethyldisilazane / tetrahydrofuran 2: tetrabutyl ammonium fluoride / tetrahydrofuran 3: hydrogen; palladium 10 on activated carbon / ethyl acetate View Scheme
参考文献
Zhang, Hong-Yan; Yamakawa, Yu-Ichiro; Matsuya, Yuji; Toyooka, Naoki; Tohda, Chihiro; Awale, Suresh; Li, Feng; Kadota, Shigetoshi; Tezuka, Yasuhiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 604 - 608
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