in neat (no solvent)
vacuum decomposition (250-300°C) of a mixture of AgNCSe and AgNCSin a glass cell; CSe2 could easily removed from the mixture by UV photodissociation at 254 nm;
参考文献
Li, Shuping; Chwee, Tsz Sian; Fan, Wai Yip
Journal of Physical Chemistry A, 2005 , vol. 109, # 51 p. 11815 - 11822
Gmelin Handbook: Se: MVol.A1, 79, page 254 - 257
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Berzelius, J. J.
Lehrbuch der Chemie, 3. Aufl., aus dem Schwedischen uebersetzt von Woehler, F., Bd. 3, Dresden-Leipzig 1834, S. 24
T=470°C; 0.666667 h; thermolysis at various temperatures; Product distribution;
参考文献
Ostroukhova, L. A.; Korchevin, N. A.; Deryagina, E. N.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 9 p. 2171 - 2172,1935 - 1936