3-氨基吡啶-2-甲酰胺合成路线 （共 17 条）
反应条件
methanesulfonic acid; triethylamine; aniline in methanol; ethanol; chloroform; acetone
参考文献
Warner-Lambert Company
Patent: US5654307 A1, 1997 ;
US 5654307 A
反应条件
hydrogen; palladium on activated charcoal in methanol; ethyl acetate P=3102.9 Torr; 144 h;
参考文献
Rewcastle, Gordon W.; Palmer, Brian D.; Thompson, Andrew M.; Bridges, Alexander J.; Cody, Donna R.; Zhou, Hairong; Fry, David W.; McMichael, Amy; Denny, William A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 9 p. 1823 - 1835
反应条件
1: 73 percent / 90percent H2SO4 / 3.5 h / 70 °C 2: H2 / Pd/C / ethyl acetate; methanol / 144 h / 3102.9 Torr View Scheme
参考文献
Rewcastle, Gordon W.; Palmer, Brian D.; Thompson, Andrew M.; Bridges, Alexander J.; Cody, Donna R.; Zhou, Hairong; Fry, David W.; McMichael, Amy; Denny, William A.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 9 p. 1823 - 1835
反应条件
hydrogenchloride; methanol Behandeln des Reaktionsprodukts mit konz. wss. NH3;
参考文献
Rasala, D.
Bulletin de la Societe Chimique de France, 1992 , # 1 p. 79 - 84
参考文献
Oakes et al.
Journal of the Chemical Society, 1956 , p. 1045,1053
反应条件
1: bromine; phosphorus (III)-bromide / 100 °C 2: iron-turnings; acetic acid / 100 °C 3: CuCN 4: H2SO4 View Scheme
参考文献
Berrie et al.
Journal of the Chemical Society, 1952 , p. 2042,2044
反应条件
1: iron-turnings; acetic acid / 100 °C 2: CuCN 3: H2SO4 View Scheme
参考文献
Berrie et al.
Journal of the Chemical Society, 1952 , p. 2042,2044
参考文献
Berrie et al.
Journal of the Chemical Society, 1952 , p. 2042,2044
反应条件
ammonium hydroxide; sodium periodate
参考文献
Oakes et al.
Journal of the Chemical Society, 1956 , p. 1045,1053
参考文献
Berrie et al.
Journal of the Chemical Society, 1952 , p. 2042,2044
