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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
50625-44-0
合成路线
(共 19 条)
120-47-8
对羟基苯甲酸乙酯
→
反应条件
50625-44-0
反应条件
1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 6 h / 100 °C 2: thionyl chloride / toluene / 3 h / Reflux View Scheme
参考文献
Lu, Huidan; Wang, Jianxiu; Song, Xiangzhi
Molecular Crystals and Liquid Crystals, 2011 , vol. 537, p. 93 - 102
112-30-1
1-癸醇
→
反应条件
50625-44-0
反应条件
1: PBr3 / Heating 2: ethanol / 7 h / Heating 3: SOCl2 / benzene / 80 °C View Scheme
参考文献
Wan, Wen; Guang, Wen-Jie; Zhao, Ke-Qin; Zheng, Wei-Zhong; Zhang, Liang-Fu
Journal of Organometallic Chemistry, 1998 , vol. 557, # 2 p. 157 - 161
154845-74-6
→
反应条件
50625-44-0
反应条件
1: potassium hydroxide / ethanol / 7 h / |Reflux 2: thionyl chloride / dichloromethane / 7 h / |Reflux View Scheme
参考文献
Singh, Sachin Kumar; Singh, Hemant Kumar; Nandi, Rajib; Kumar, Vijay; Tarcea, Nicolae; Popp, Juergen; Singh, Ranjan K.; Singh, Bachcha
Polyhedron, 2014 , vol. 74, p. 99 - 112
50625-44-0
→
反应条件
123436-82-8
4-羟基苯基4-(十二基氧基)苯甲酸盐
反应条件
1: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice 2: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
50625-44-0
→
反应条件
82052-58-2
反应条件
1: water; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / dichloromethane / 12 h 2: Jone's reagent / acetone / 20 °C 3: thionyl chloride / 3 h / 100 °C View Scheme
参考文献
Majumdar; Ghosh; Chakravorty
Molecular Crystals and Liquid Crystals, 2010 , vol. 533, p. 63 - 72
50625-44-0
+
99-93-4
对羟基苯乙酮
→
反应条件
55097-88-6
反应条件
pyridine Cooling with iceHeating;
参考文献
Thaker; Patel; Kanojiya
Molecular Crystals and Liquid Crystals, 2009 , vol. 509, # 1 p. 145 - 164
50625-44-0
+
123-08-0
对羟基苯甲醛
→
反应条件
56800-35-2
反应条件
in pyridine; benzene 12 h, 25 deg C; 1 h, 80 deg C; Yield given;
参考文献
Dave, Jayrang S.; Menon, Meera R.; Patel, Pratik R.
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 364, p. 575 - 587
Title/Abstract Full Text View citing articles Show Details
Prajapati; Sharma; Chudgar
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 364, p. 815 - 823
50625-44-0
+
767-00-0
4-羟基苯甲腈
→
反应条件
59874-09-8
反应条件
pyridine Ambient temperature;
参考文献
Serrano, Jose Luis; Sierra, Teresa; Gonzalez, Yolanda; Bolm, Carsten; Weickhardt, Konrad; Magnus, Angelika; Moll, Guido
Journal of the American Chemical Society, 1995 , vol. 117, # 32 p. 8312 - 8321
100-02-7
对硝基苯酚
+
50625-44-0
→
反应条件
63635-84-7
4-硝基苯基 4-癸氧基苯甲酸酯
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C;
参考文献
Majumdar, Krishna C.; Chattopadhyay, Buddhadeb; Chakravorty, Santanu; Pal, Nilasish; Sinha, Randhir Kumar
Tetrahedron Letters, 2008 , vol. 49, # 50 p. 7149 - 7152
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