6(4-溴苯基)-3(2H)吡嗪酮合成路线 （共 9 条）
反应条件
bromine in acetic acid
T=20 - 100°C; 1 h;
参考文献
ABBOTT LABORATORIES
Patent: WO2006/65233 A1, 2006 ;
Location in patent: Page/Page column 75-76 ;
反应条件
hydrazine hydrate in ethanol
10 h; Reflux;
参考文献
El-Mobayed, Medhat M.; Hussein, Ahmed M.; Mohlhel, Wafia M.
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 3 p. 534 - 537
反应条件
hydrazine hydrate in ethanol
3 h; Reflux;
参考文献
El-Hashash; El-Sayed; El-Kady; Mohamed
Egyptian Journal of Chemistry, 2008 , vol. 51, # 1 p. 103 - 112
反应条件
hydrazine hydrate in ethanol
4 h; Reflux;
参考文献
El-Hashash; El-Sayed; El-Kady; Mohamed
Egyptian Journal of Chemistry, 2008 , vol. 51, # 1 p. 103 - 112
反应条件
hydrazine hydrate
5 h; Heating;
参考文献
Kolos; Kovalenko; Borovskoy
Chemistry of Heterocyclic Compounds, 2011 , vol. 47, # 8 p. 983 - 988
反应条件
1: ethanol / 4 h / Reflux
2: hydrazine hydrate / 5 h / Heating
View Scheme
参考文献
Kolos; Kovalenko; Borovskoy
Chemistry of Heterocyclic Compounds, 2011 , vol. 47, # 8 p. 983 - 988
反应条件
trichlorophosphate
T=100°C; 16 h;
参考文献
ABBOTT LABORATORIES
Patent: WO2006/65233 A1, 2006 ;
Location in patent: Page/Page column 76 ;
反应条件
in trichlorophosphate
参考文献
American Cyanamid Company
Patent: US4092311 A1, 1978 ;
反应条件
ethylenediamine in N-methyl-acetamide; water
参考文献
American Cyanamid Company
Patent: US4092311 A1, 1978 ;
