4-吲哚吡啶-2,6-二羧酸合成路线 （共 8 条）
反应条件
1: 89 percent / NaBH4 / ethanol 2: 64 percent / PBr3 / CHCl3 / Heating View Scheme
参考文献
Takalo, Harri; Pasanen, Paavo; Kankare, Jouko
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 6 p. 373 - 377
反应条件
sodium tetrahydroborate in ethanol
参考文献
Takalo, Harri; Pasanen, Paavo; Kankare, Jouko
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 6 p. 373 - 377
反应条件
hydrogen iodide; potassium iodide in water
T=130°C;
参考文献
Pauvert, Mickael; Laine, Patrick; Jonas, Marco; Wiest, Olaf
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 543 - 548
反应条件
potassium hydroxide in methanol; dichloromethane
T=20°C; 7 h;
参考文献
Nakamura, Tatsuya; Mizukami, Shin; Tanaka, Miho; Kikuchi, Kazuya
Chemistry - An Asian Journal, 2013 , vol. 8, # 11 p. 2685 - 2690
反应条件
orthophosphorus acid; hydrogen iodide
5 h; Heating;
参考文献
Storm, Ole; Luening, Ulrich
European Journal of Organic Chemistry, 2002 , # 21 p. 3680 - 3685
反应条件
1.1: phosphorus pentachloride / water; tetrachloromethane / 15 h / |Reflux
1.2: 4 h / |Reflux
2.1: acetyl chloride; sodium iodide / acetonitrile / 10 h / 0 - 50 °C / |Inert atmosphere; |Sonication
3.1: potassium hydroxide / dichloromethane; methanol / 7 h / 20 °C
View Scheme
参考文献
Nakamura, Tatsuya; Mizukami, Shin; Tanaka, Miho; Kikuchi, Kazuya
Chemistry - An Asian Journal, 2013 , vol. 8, # 11 p. 2685 - 2690
反应条件
phosphorus; hydrogen iodide
参考文献
Graf
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 148, p. 13,16
反应条件
1: 70 percent / sulfuric acid / 4 h / Heating
2: 70 percent / sodium borohydride / methanol / 17 h / Heating
3: 90 percent / selenium dioxide / dioxane / 5.5 h / Heating
View Scheme
参考文献
Storm, Ole; Luening, Ulrich
European Journal of Organic Chemistry, 2002 , # 21 p. 3680 - 3685
