对戊基苯基-4-辛氧基苯甲酸酯合成路线 (共 8 条)
反应条件
1: ethanol / Heating
2: thionyl chloride / 2 h / Heating
3: pyridine / Ambient temperature
View Scheme
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
1: 1.) hydrazine hydrate, 2.) KOH / 1.) diethylene glycol, reflux, 1h; 2.) reflux, 1h
2: pyridine / Ambient temperature
View Scheme
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
1: thionyl chloride / 2 h / Heating
2: pyridine / Ambient temperature
View Scheme
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
1: AlCl3 / CH2Cl2 / 1.) 0 deg C, 30 min; 0 deg C, 30 min; 2.) room temperature, overnight
2: 1.) hydrazine hydrate, 2.) KOH / 1.) diethylene glycol, reflux, 1h; 2.) reflux, 1h
3: pyridine / Ambient temperature
View Scheme
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
1: ethanol / Heating
2: thionyl chloride / 2 h / Heating
3: pyridine / Ambient temperature
View Scheme
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
1: AlCl3 / CH2Cl2 / 1.) 0 deg C, 30 min; 0 deg C, 30 min; 2.) room temperature, overnight
2: 1.) hydrazine hydrate, 2.) KOH / 1.) diethylene glycol, reflux, 1h; 2.) reflux, 1h
3: pyridine / Ambient temperature
View Scheme
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
in pyridine
Ambient temperature;
参考文献
Malthete, Jacques; Canceill, Josette; Gabard, Jacqueline; Jacques, Jean
Tetrahedron, 1981 , vol. 37, # 16 p. 2815 - 2821
反应条件
dicyclohexyl-carbodiimide
1 h; Heating;
参考文献
Neubert, Mary E.; Jirousek, Michael R.; Hanlon, Carol A.
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 133, p. 223 - 234