异硫氰酸 2-氯苯甲酰脂合成路线 (共 11 条)
反应条件
PEG-400 in ethyl acetate T=20°C;
参考文献
Wei, Tai-Bao; Li, Man-Lin; Lin, Qi; Liu, Hong; Zhang, You-Ming
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 7 p. 1583 - 1592
反应条件
tetrabutylammomium bromide in water; benzene 2 h; Ambient temperature;
参考文献
Reeves, W. Preston; Simmons, Art; Rudis, John A.; Bothwell, Tim C.
Synthetic Communications, 1981 , vol. 11, # 10 p. 781 - 786
反应条件
PEG-400 in ethyl acetate T=20°C;
参考文献
Li, Man-Lin; Zhang, You-Ming; Wei, Tai-Bao
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 3 p. 544 - 549
参考文献
Celamerck GmbH and Co. KG
Patent: US4457943 A1, 1984 ;
参考文献
Pete, Umesh D.; Zade, Chetan M.; Bhosale, Jitendra D.; Tupe, Santosh G.; Chaudhary, Preeti M.; Dikundwar, Amol G.; Bendre, Ratnamala S.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 17 p. 5550 - 5554
反应条件
1: SOCl2 / Heating 2: PEG-600 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Rajak, Harish; Behera, Chinmay K.; Pawar, Rajesh S.; Singour, Pradeep K.; Kharya, Murli Dhar
Chinese Chemical Letters, 2010 , vol. 21, # 10 p. 1149 - 1152
反应条件
in acetone T=45 - 50°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Cho; Shon; Parkanyi
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 7 p. 1645 - 1649
反应条件
in acetone T=20°C; 2 h;
参考文献
Emen; Arslan; Kuelcue; Floerke; Duran
Polish Journal of Chemistry, 2005 , vol. 79, # 10 p. 1615 - 1626
反应条件
ammonia in dichloromethane
T=0 - 20°C;
参考文献
Yoo, Choong Leol; Yu, Gui Jun; Yang, Baoxue; Robins, Lori I.; Verkman; Kurth, Mark J.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 8 p. 2610 - 2614
反应条件
tetraphosphorus decasulfide in xylene
Heating;
参考文献
Derocque,J.-L.; Vialle,J.
Bulletin de la Societe Chimique de France, 1966 , p. 1183 - 1186