4-氰基-4'-甲基联苯合成路线 （共 60 条）
反应条件
in tetrahydrofuran T=90°C; Inert atmosphere;
参考文献
Minami, Hiroki; Wang, Xuan; Wang, Chao; Uchiyama, Masanobu
European Journal of Organic Chemistry, 2013 , # 35 p. 7891 - 7894
反应条件
1: SbF3 2: 67 percent / KF / (η3-C3H5PdCl)2 / dimethylformamide / 21 h / 100 °C View Scheme
参考文献
Hatanaka, Yasuo; Fukushima, Satoshi; Hiyama, Tamejiro
Chemistry Letters, 1989 , p. 1711 - 1714
反应条件
1.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / |Inert atmosphere 1.2: -78 - 0 °C 2.1: tetrahydrofuran / 90 °C / |Inert atmosphere View Scheme
参考文献
Minami, Hiroki; Wang, Xuan; Wang, Chao; Uchiyama, Masanobu
European Journal of Organic Chemistry, 2013 , # 35 p. 7891 - 7894
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 2 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 2 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 2 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 3 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 3.5 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran 1 h; Heating;
参考文献
Miller, Joseph A.; Farrell, Robert P.
Tetrahedron Letters, 1998 , vol. 39, # 36 p. 6441 - 6444
反应条件
1: PdCl2(dppf) / tetrahydrofuran; diethyl ether / 20 °C 2: 89 percent / PhPdI(PPh3)2 / dimethylformamide / 2 h / Heating View Scheme
参考文献
Bumagin, N. A.; Luzikova, E. V.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1480 - 1486
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1650 - 1656
