4-氯-n-(2-氯乙酰基)苯碳酰肼合成路线 （共 5 条）
反应条件
in acetonitrile T=20°C;
参考文献
OSLO UNIVERSITY HOSPITAL HF; HOLSWORTH, Dan; WAALER, Jo; MACHON, Ondrej; KRAUSS, Stefan; GOLDING, Louise
Patent: WO2010/139966 A1, 2010 ;
Location in patent: Page/Page column 89-90 ;
反应条件
1: chloroacetic acid With 2,6-dimethylpyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate in dichloromethane T=25°C; 0.166667 h; 2: 4-chlorobenzoic acid hydrazide T=20°C; 3 h;
参考文献
Gurupadaswamy, Handuvinahalli Devanna; Girish, Virupaksha; Zameer, Farhan; Hegdekatte, Raghavendra; Chauhan, Jyoti Bala; Khanum, Shaukath Ara
Archiv der Pharmazie, 2013 , vol. 346, # 11 p. 805 - 811
反应条件
1: N2H4*H2O 2: tetrahydrofuran View Scheme
参考文献
Cao, Song; Qian, Xuhong; Song, Gonghua; Chai, Bing; Jiang, Zhisheng
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 1 p. 152 - 155
反应条件
1.1: SOCl2 1.2: CH3CO2Et; NH2-NH2*H2O View Scheme
参考文献
Moger, Manjunath; Satam, Vijay; Govindaraju, Darshan Raj C.; Paniraj; Gopinath, Vadiraj S.; Hindupur, Rama Mohan; Pati, Hari N.
Journal of the Brazilian Chemical Society, 2014 , vol. 25, # 1 p. 104 - 111
反应条件
trichlorophosphate in acetonitrile 16 h; Reflux;
参考文献
OSLO UNIVERSITY HOSPITAL HF; HOLSWORTH, Dan; WAALER, Jo; MACHON, Ondrej; KRAUSS, Stefan; GOLDING, Louise
Patent: WO2010/139966 A1, 2010 ;
Location in patent: Page/Page column 89-90 ;
