2,5-二甲基-1-苯乙基-1H-吡咯合成路线 (共 2 条)
反应条件
amberlite IR 120 acidic resin
T=20°C; Paal-Knorr pyrrole synthesis; 0.233333 h; Neat (no solvent);
参考文献
Devi, Aarti; Shallu; Sharma; Singh, Jasvinder
Synthetic Communications, 2012 , vol. 42, # 10 p. 1480 - 1488
反应条件
1: hex-3-yne-2,5-diol With ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene
0.5 h; Inert atmosphereReflux;
2: phenethylamine in toluene
23.5 h; Inert atmosphereReflux;
参考文献
Pridmore, Simon J.; Slatford, Paul A.; Taylor, James E.; Whittlesey, Michael K.; Williams, Jonathan M.J.
Tetrahedron, 2009 , vol. 65, # 44 p. 8981 - 8986