3-(4-氯苯基)-2-(苯磺酰基)丙烯腈合成路线 (共 4 条)
反应条件
[C4mim][OH] in ethanol 6 h; RefluxGreen chemistry; SolventTimeReagent/catalyst;
参考文献
Zhang, Lei; Ding, Mao Hua; Guo, Hong Yun
Chinese Chemical Letters, 2012 , vol. 23, # 12 p. 1352 - 1354
反应条件
piperidine; acetic acid in toluene 24 h; RefluxDean-Stark;
参考文献
Rajkumar, Sundaram; Shankland, Kenneth; Goodman, Jonathan M.; Cobb, Alexander J. A.
Organic Letters, 2013 , vol. 15, # 6 p. 1386 - 1389
反应条件
1: dimethylformamide 2: piperidine / benzene; dimethylformamide View Scheme
参考文献
Beck,G.; Guenther,D.
Chemische Berichte, 1973 , vol. 106, p. 2758 - 2766
反应条件
samarium diiodide in tetrahydrofuran; methanol T=60°C; Reduction; desulfonylation; 4 h;
参考文献
Guo, Hongyun; Zhang, Yongmin
Synthetic Communications, 2000 , vol. 30, # 11 p. 1879 - 1885