3-巯基-3-甲基-1-丁醇乙酸酯合成路线 (共 4 条)
反应条件
hydrogenchloride in methanol; diethyl ether
参考文献
Polak's Frutal Works B.V.; Douwe Egberts Koninklijke Tabaksfabriek-Koffiebranderijen-Theehandel N.V.
Patent: US3970689 A1, 1976 ;
反应条件
sodium tetrahydroborate; NaOCH3; sodium chloride in methanol; water
参考文献
Polak's Frutal Works B.V.; Douwe Egberts Koninklijke Tabaksfabriek-Koffiebranderijen-Theehandel N.V.
Patent: US3970689 A1, 1976 ;
反应条件
in dichloromethane
T=22°C; 18 h;
参考文献
Starkenmann, Christian; Niclass, Yvan; Escher, Sina
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 11 p. 4511 - 4517
反应条件
sodium sulfate in dichloromethane
T=20°C; Acetylation; 18 h;
参考文献
Tominaga, Takatoshi; Dubourdieu, Denis
Journal of Agricultural and Food Chemistry, 2000 , vol. 48, # 7 p. 2874 - 2876