2,3-二甲基-2,3-环氧丁烷合成路线 (共 115 条)
反应条件
sodium perchlorate; water T=35°C; kinetic isotope effect; Rate constant;
参考文献
Pocker, Y.; Ronald, B. P.; Anderson, K. W.
Journal of the American Chemical Society, 1988 , vol. 110, # 19 p. 6492 - 6497
反应条件
T=150°C; im Druckrohr;
参考文献
Delacre
Bulletin de la Societe Chimique de France, 1908 , vol. <4> 3, p. 209
反应条件
durch Perchlorsaeure katalysierte Reaktion;
参考文献
Pocker
Chemistry and Industry (London, United Kingdom), 1959 , p. 332
反应条件
water; ammonium thiocyanate T=40°C; 34 h;
参考文献
Kleiner, Christian M.; Horst, Luise; Wuertele, Christian; Wende, Raffael; Schreiner, Peter R.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 7 p. 1397 - 1403
反应条件
2-(Phenylsulfonyl)-3-(p-nitrophenyl)oxaziridine; (5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride in dichloromethane
T=25°C; 2 h;
参考文献
Yuan, Lung-Chi; Bruice, Thomas C.
Journal of the Chemical Society, Chemical Communications, 1985 , # 13 p. 868 - 869
反应条件
dihydrogen peroxide in various solvent(s)
T=22°C; Epoxidation; hydroxylation; 20 h;
参考文献
Neimann, Karine; Neumann, Ronny
Organic Letters, 2000 , vol. 2, # 18 p. 2861 - 2863
反应条件
1:
2: 2,3-dimethylbutane-2,3-diol With [EMIM][HSO4]
T=140°C;
参考文献
Ignatyev, Nikolai (Mykola); Welz-Biermann, Urs; Koppe, Karsten; Barthen, Peter; Frohn, Hermann Josef
Patent: US2009/62571 A1, 2009 ;
Location in patent: Page/Page column 9 ;
反应条件
5,10,15,20-tetrakis(2',6'-dichlorophenyl)-β-octabromoporphyrin; oxygen; hexacarbonyl molybdenum in dichloromethane
T=30°C; P=760.051 Torr; 0.75 h; Irradiation;
参考文献
Campestrini, Sandro; Tonellato, Umberto
European Journal of Organic Chemistry, 2002 , # 22 p. 3827 - 3832
反应条件
tert.-butylhydroperoxide; silica gel; β-MoO3 in decane
T=50°C; 12 h; Yield given. Yields of byproduct given;
参考文献
Juwiler, David; Blum, Jochanan; Neumann, Ronny
Chemical Communications, 1998 , # 10 p. 1123 - 1124
反应条件
tetramethyl-1,2-dioxetane chemienergization in hexane
T=60°C;
参考文献
Adam, Waldemar; Cueto, Omar; Guedes, Luis N.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2106 - 2107