2,3-二甲基-2,3-环氧丁烷合成路线 (共 115 条)
反应条件
in benzene-d6
Heating;
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.
Journal of Organic Chemistry, 1984 , vol. 49, p. 793 - 798
反应条件
ozone
P=4.1 Torr; 0.000777778 h; reaction in gas phase; mass spectrum of ozone and title compound; Product distributionMechanism;
参考文献
Martinez, Richard I.; Herron, John T.; Huie, Robert E.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3807 - 3820
反应条件
1: lead smoothness / 220 - 230 °C
2: hypochlorous acid
3: solid potassium hydroxide
View Scheme
参考文献
Eltekow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1882 , vol. 14, p. 368
Chemische Berichte, 1883 , vol. 16, p. 397
反应条件
ozone
T=-254.16 - -238.16°C; 19 h; IrradiationInert atmosphere;
参考文献
Coleman, Bridgett E.; Ault, Bruce S.
Journal of Physical Chemistry A, 2010 , vol. 114, # 48 p. 12667 - 12674
反应条件
dichloromethane; sodium carbonate; acetic acid
参考文献
Du Pont de Nemours and Co.
Patent: US2838524 , 1955 ;
反应条件
in dichloromethane
Kinetics; temp., 0°C; Mo complex, 0.02 M; solvent, CH2Cl2; olefin/complex = 40; pptn. with Et2O;
参考文献
Chaumette, Patrick; Mimoun, Hubert; Saussine, Lucien; Fischer, Jean; Mitschler, Andre
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 291 - 310
反应条件
Diethyloxytriphenylphosphorane
1.) C6D6, 7 d, reflux; 2.) 200 deg C, 15 torr; various solvent, temperature, time; Product distribution;
参考文献
Robinson, Philip L.; Barry, Carey N.; Kelly, Jeffery W.; Evans, Slayton A.
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5210 - 5219
反应条件
in chloroform
T=34°C; Rate constant;
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1939 - 1942
反应条件
in benzene-d6
T=34°C; Rate constant;
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1939 - 1942
反应条件
in chloroform
T=34°C; Rate constant;
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1939 - 1942