1: (m-Br-C6H4)PPh2 With n-butyllithium in tetrahydrofuran
T=-78°C; 0.5 h;
2: N,N-dimethyl-formamide in tetrahydrofuran
T=-78 - 20°C; Further stages.;
参考文献
Van Leeuwen, Piet W. N. M.; Rivillo, David; Raynal, Matthieu; Freixa, Zoraida
Journal of the American Chemical Society, 2011 , vol. 133, # 46 p. 18562 - 18565
1.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
View Scheme
参考文献
Van Leeuwen, Piet W. N. M.; Rivillo, David; Raynal, Matthieu; Freixa, Zoraida
Journal of the American Chemical Society, 2011 , vol. 133, # 46 p. 18562 - 18565
1.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
View Scheme
参考文献
Van Leeuwen, Piet W. N. M.; Rivillo, David; Raynal, Matthieu; Freixa, Zoraida
Journal of the American Chemical Society, 2011 , vol. 133, # 46 p. 18562 - 18565
