N,N-二甲基-2,3-二氯丙胺盐酸盐合成路线 (共 14 条)
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; propane-1-thiol; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min, 2) H2O, CHCl3, 3 h; Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride multistep reaction; reaction of organo-thiosulfates (BUNTE-salts) with mercaptans; other mercaptans; Mechanism;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 5 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride multistep reaction; reaction of organo-thiosulfates (BUNTE-salts) with mercaptans; other mercaptans; Mechanism;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 7 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 6 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 5 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847
反应条件
sodium hydroxide; sodium thiosulfate; sodium chloride 1) EtOH, H2O, reflux, 30 min., 2) H2O, CHCl3, 7 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Muehlstaedt, M.; Heinicke, J.; Schubert H.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 6 p. 841 - 847